反应条件
1: 277 mg / DIBAL-H / toluene / 1 h / -74 °C 2: 71.2 percent / 4-methylmorpholine-N-oxide, tetrapropyl-ammonium perruthenate, molecular sieves 4 Angstroem / CH2Cl2 / 2 h 3: 71.3 percent / acetonitrile / 14 h / Heating 4: 13 g / HF / acetonitrile / 1.5 h / Ambient temperature View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 2 p. 437 - 444
