4-(烯丙氧基)-1-丁醇合成路线 (共 8 条)
反应条件
potassium hydroxide in tetrahydrofuran 0.5 h; Heating;
参考文献
Toepfer; Toepfer, Alexander; Kretzschmar; Kretzschmar, Gerhard; Bartnik; Bartnik, Eckart
Tetrahedron Letters, 1995 , vol. 36, # 50 p. 9161 - 9164
反应条件
zirconium tetrachloride in acetonitrile T=20°C; 0.5 h;
参考文献
Sharma; Srinivas; Radha Krishna, Palakodety
Tetrahedron Letters, 2003 , vol. 44, # 25 p. 4689 - 4691
反应条件
methanol; Montmorillonite K-10 clay T=20°C; Methanolytic deprotection;
参考文献
Taniguchi, Takahiko; Kadota, Kohei; Elazab, Adel S.; Ogasawara, Kunio
Synlett, 1999 , # 8 p. 1247 - 1248
反应条件
sodium in toluene 24 h;
参考文献
Krompiec; Antoszczyszyn; Urbala; Bieg
Polish Journal of Chemistry, 2000 , vol. 74, # 5 p. 737 - 739
反应条件
oxygen; ω-hydroxylase from Pseudomonas oleovorans T=30°C; 12 h; P1 medium for bacteria growth; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fu, Hong; Shen, Gwo-Jenn; Wong, Chi-Huey
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 5 p. 167 - 170
反应条件
dirhodium tetraacetate; hydrogen; diethylphosphinoethane in ethanol T=120°C; P=30400 Torr; 4 h; hydrocarbonylation; Product distribution;
参考文献
Simpson, Michael C.; Currie, Alan W. S.; Andersen, Jo-Ann M.; Cole-Hamilton, David J.; Green, Michael J.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 9 p. 1793 - 1800
反应条件
1: 19.9 g / Jones reagent / acetone; H2O / cooling
2: oxalyl chloride / hexane / 3 h / 20 °C
View Scheme
参考文献
Harmata, Michael; Rashatasakhon, Paitoon; Barnes, Charles L.
Canadian Journal of Chemistry, 2006 , vol. 84, # 10 p. 1456 - 1469
反应条件
tris(triphenylphosphine)ruthenium(II) chloride
T=120°C; 4 h;
参考文献
Urbala, Magdalena; Kuznik, Nikodem; Krompiec, Stanislaw; Rzepa, Jozef
Synlett, 2004 , # 7 p. 1203 - 1206