甲基4-(壬氧基)苯甲酸酯合成路线 （共 4 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide 20 h; Inert atmosphereReflux;
参考文献
Khairuddean, Melati; Twieg, Robert J.
Molecular Crystals and Liquid Crystals, 2009 , vol. 503, # 1 p. 3 - 31
反应条件
sodium hydride 1.) THF, 0 deg C, 2.) reflux, 4 h; Multistep reaction;
参考文献
Nakai; Konno; Kosuge; Sakuyama; Toda; Arai; Obata; Katsube; Miyamoto; Okegawa; Kawasaki
Journal of Medicinal Chemistry, 1988 , vol. 31, # 1 p. 84 - 91
反应条件
1: With potassium hydroxide in tetrahydrofuran; ethanol; water Reflux; 2: in tetrahydrofuran; ethanol; water T=20°C; Acidic aq. solution;
参考文献
Khairuddean, Melati; Twieg, Robert J.
Molecular Crystals and Liquid Crystals, 2009 , vol. 503, # 1 p. 3 - 31
反应条件
1.1: potassium hydroxide / tetrahydrofuran; ethanol; water / Reflux
1.2: 20 °C / Acidic aq. solution
2.1: oxalyl dichloride / dichloromethane / 8 h / 40 °C
View Scheme
参考文献
Yang, Hong; Lv, You-Jing; Lin, Bao-Ping; Zhang, Xue-Qin; Sun, Ying; Guo, Ling-Xiang
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 8 p. 1086 - 1098
