carbon in neat (no solvent)
mixture of U3O8 and coal (4:1), passing over of a stream of Cl, forming of UCl4;; proportions (see above) are used to inhibit forming of compd., which contain C;;
carbon in neat (no solvent)
on passing dry Cl over a moderately heated mixture of coal and uranyl chloride; UCl5 is found in two forms, depending on velocity of stream of Cl; UCl5 is condensing more distant from the heated place than UCl4;;
in neat (no solvent)
react. only proceeds at red heat completely; formed UCl4 is sublimating off quantitatively; using sufficient amt. of S2Cl2 inhibits simultaneous formation of UO2Cl2;;
Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
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Brendan Timmons, R.
Diss. Abstr., Diss. Catholic Univ. of America 1963, S. 1/68 1965 , vol. 26, p. 736
