2,2,4-三甲基-1,2-二氢喹啉合成路线 (共 35 条)
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate; ytterbium(III) triflate T=20°C; 0.5 h;
参考文献
Li, Yongshu; Wu, Chunlei; Huang, Jianliang; Su, Weike
Synthetic Communications, 2006 , vol. 36, # 20 p. 3065 - 3073
反应条件
indium(III) chloride; silica gel 0.333333 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Hajra, Alakananda; Dey, Suvendu S.; Jana, Umasish
Tetrahedron, 2003 , vol. 59, # 6 p. 813 - 819
反应条件
tetrafluoroboric acid diethyl ether complex; tri-ruthenium(0)dodecacarbonyl in benzene T=95°C; 24 h;
参考文献
Yi, Chae S.; Yun, Sang Young
Journal of the American Chemical Society, 2005 , vol. 127, # 48 p. 17000 - 17006
反应条件
iodine in acetone T=30°C; 12 h; Green chemistry; regioselective reaction;
参考文献
RSC Advances, , vol. 4, # 12 p. 6267 - 6274
反应条件
toluene-4-sulfonic acid in toluene T=110°C; 120 h;
参考文献
Leis, Jaan; Pihl, Aino; Pihlaja, Kalevi; Karelson, Mati
ACH - Models in Chemistry, 1998 , vol. 135, # 4 p. 573 - 581
反应条件
aniline hydrochloric acid T=180°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 46, # 22 p. 4552 - 4555
反应条件
1: sulfuric acid; nitric acid / chloroform; benzene / 5 h / 50 °C / |Industrial scale 2: hydrogen / 200 °C / |Industrial scale 3: hydrogenchloride / 6 h / 140 °C View Scheme
反应条件
in 1,4-dioxane T=20°C; 12 h; UV-irradiation;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 41, # 7 p. 936 - 937
反应条件
bei laengerem Kochen;
参考文献
Chemische Berichte, , vol. 65, p. 1514
Chemische Berichte, , vol. 55, p. 1918
Journal of the Chemical Society, , p. 1327
Journal of the American Chemical Society, , vol. 55, p. 2805
Chemische Berichte, , vol. 54, p. 1726;
Chemische Berichte, , vol. 56, p. 2416
反应条件
1: ammonia / 450 °C / 760.05 Torr / |Industrial scale 2: hydrogenchloride / 6 h / 140 °C View Scheme