mixt. of 1,2-dicyanobenzene and quinoline was heated to 140°C under N2 with stirring, CuCl2 was added, heated at 160-190°C for 3-5h; filtered, washed with DMF, sublimed;
参考文献
Solid State Communications, , vol. 118, # 12 p. 633 - 638
aluminium trichloride; sodium chloride in melt at 200°C;;
参考文献
Borodkin, V. F.; Usacheva, K. V.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1956 , vol. 29, p. 1383 - 1386
C., 1959 , p. 14663
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Gmelin Handbook: Cu: MVol.B4, 145, page 1768 - 1770
K in neat (no solvent)
byproducts: potassium phthalocyanine; under Ar, glovebox; Cu compd. placed into one end of tube at 450°C; K was introduced at other end at 200°C;
参考文献
Margadonna, Serena; Prassides, Kosmas; Iwasa, Yoshihiro; Taguchi, Yasujiro; Craciun, Monica F.; Rogge, Sven; Morpurgo, Alberto F.
Inorganic Chemistry, 2006 , vol. 45, # 26 p. 10472 - 10478
