2,6-二甲氧基苯甲酸合成路线 （共 118 条）
反应条件
sulfuryl dichloride in chloroform 0.5 h; Heating;
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
反应条件
1: potassium tert-butylate / ethanol / 20 °C 2: oxygen; copper diacetate; silver carbonate / N,N-dimethyl-formamide / 18 h / 145 °C View Scheme
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Journal of the American Chemical Society, 2012 , vol. 134, # 24 p. 9938 - 9941
反应条件
bromine in acetic acid 1.5 h;
参考文献
Cuyegkeng, Maria Assunta; Mannschreck, Albrecht
Chemische Berichte, 1987 , vol. 120, p. 803 - 810
反应条件
diethylamino-sulfur trifluoride in dichloromethane T=0 - 5°C; 0.25 h;
参考文献
Mukherjee, Jogeshwar
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 151 - 154
反应条件
oxygen; palladium diacetate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; Heck reaction; P=1368.09 Torr; 10 h; optical yield given as percent dediastereoselective reaction;
参考文献
Fu, Zhengjiang; Huang, Shijun; Su, Weiping; Hong, Maochun
Organic Letters, 2010 , vol. 12, # 21 p. 4992 - 4995
反应条件
4-diphenylaminobenzene; oxygen; palladium diacetate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 24 h; Molecular sieve; optical yield given as percent de;
参考文献
Fu, Zhengjiang; Huang, Shijun; Kan, Jian; Su, Weiping; Hong, Maochun
Dalton Transactions, 2010 , vol. 39, # 47 p. 11317 - 11321
反应条件
palladium (II) trifluoroacetate; 6-mbipy in water T=100°C; 48 h;
参考文献
Lindh, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Angewandte Chemie - International Edition, 2010 , vol. 49, # 42 p. 7733 - 7737
反应条件
1: palladium (II) trifluoroacetate; 6-mbipy; p-benozquinone / N,N-dimethyl-formamide / 24 h / 120 °C 2: hydrogenchloride; water / 2 h / 20 °C View Scheme
参考文献
Fardost, Ashkan; Lindh, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 870 - 878
反应条件
1: BH3 / tetrahydrofuran / 2 h / Heating 2: 4 percent / H2O / 0.17 h / Irradiation View Scheme
参考文献
Wan, Peter; Chak, Becky
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 1751 - 1756
反应条件
1: 60 percent / SO2Cl2 / CHCl3 / 0.5 h / Heating 2: SOCl2 / 0.23 h / Heating View Scheme
参考文献
Florvall, Lennart; Oegren, Sven-Ove
Journal of Medicinal Chemistry, 1982 , vol. 25, # 11 p. 1280 - 1286
