2,6-二甲氧基苯甲酸合成路线 （共 118 条）
反应条件
1: 1,3-dimethoxy benzene With sodium 2: carbon dioxide
参考文献
US6384273 B1, ;
Page column 7-8 ;
反应条件
1: chlorobenzene; 1,3-dimethoxy benzene With sodium in toluene T=20°C; 2: carbon dioxide in toluene T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 2 p. 340 - 343
反应条件
potassium hydroxide in dimethyl sulfoxide T=110°C; 4 h;
参考文献
Synthetic Communications, , vol. 22, # 1 p. 13 - 22
反应条件
1: With AlCl3, aluminium chloride in dichloromethane T=-15 - 20°C; 5 h; Inert atmosphereLarge scale; 2: With hydrogenchloride in dichloromethane; water T=25°C; Inert atmosphereLarge scale;
参考文献
Organic Process Research and Development, , vol. 8, # 6 p. 897 - 902
反应条件
water; InI3; silica gel Hydrolysis; 1 h; Heating;
参考文献
Synthetic Communications, , vol. 30, # 22 p. 4167 - 4171
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Synthesis, , # 4 p. 594 - 596
反应条件
hydrogenchloride in water; acetic acid 4 h; Heating;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 102, # 8 p. 557 - 564
反应条件
Ph2Mg; sodium 2-ethoxyethoxide in benzene T=65°C; 5.5 h;
参考文献
Journal of Organometallic Chemistry, , vol. 290, p. 1 - 14
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 42, # 9 p. 1709 - 1712
反应条件
n-butyllithium; diethyl ether anschliessend Erwaermen mit Kohlendioxid;
参考文献
Journal of the American Chemical Society, , vol. 62, p. 667
Chemische Berichte, , vol. 72, p. 89,91
