5,13-二甲基-1,9-二氮杂四环[7.7.1.02,7.010,15]十七碳-2,4,6,10,12,14-六烯合成路线 （共 3 条）
反应条件
resolving agent: trans-cellulose tris(4-phenylazophenylcarbamate) ( CPAPC ) adsorbed on silica gel; optical resolution degree examined by HPLC on cis/trans-CPAPC;
参考文献
RUDJER BOSKOVIC INSTITUTE
Patent: WO2009/109792 A1, 2009 ;
Location in patent: Page/Page column 16; Figure 5 ;
反应条件
1: 73 percent / AlCl3 / CH2Cl2 / 8 h / 25 °C View Scheme
参考文献
Satishkumar, Sakilam; Periasamy, Mariappan
Tetrahedron Asymmetry, 2006 , vol. 17, # 7 p. 1116 - 1119
反应条件
1: 1,2-dichloro-ethane / 120 h / 45 - 50 °C / |Resolution of racemate 2: sodium carbonate / dichloromethane; water View Scheme
参考文献
Jameson, Donald L.; Field, Thomas; Schmidt, Monica R.; Destefano, Alyson K.; Stiteler, Christopher J.; Venditto, Vincent J.; Krovic, Brooke; Hoffman, Christopher M.; Ondisco, Matthew T.; Belowich, Matthew E.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11590 - 11596
