4-(三氟甲基)苯基三氟甲烷磺酸酯合成路线 （共 13 条）
反应条件
pyridine T=0 - 20°C; 48 h;
参考文献
Gill, Duncan; Hester, Alison J.; Lloyd-Jones, Guy C.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 17 p. 2547 - 2548
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide in N,N-dimethyl-formamide T=70°C;
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
反应条件
1: 82 percent / Et3N / CH2Cl2 2: 88 percent / CuI, HMPA / dimethylformamide / 70 °C View Scheme
参考文献
Qing, Feng-Ling; Fan, Junfa; Sun, Hong-Bin; Yue, Xiang-Jun
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 20 p. 3053 - 3057
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrolytic reduction;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
pyridine; hydrogen; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide T=80°C; P=15001.5 Torr; 60 h;
参考文献
Brennfuhrer, Anne; Neumann, Helfried; Beller, Matthias
Synlett, 2007 , # 16 p. 2537 - 2540
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; electrolytic reduction;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=60°C; electrochemical reduction;
参考文献
Jutand, Anny; Negri, Serge; Mosleh, Adil
Journal of the Chemical Society, Chemical Communications, 1992 , # 23 p. 1729 - 1730
反应条件
diisobutylaluminium hydride; bis(acetylacetonate)nickel(II); triphenylphosphine in ethylene glycol dimethyl ether; hexane T=80°C; 6 h;
参考文献
Shirakawa, Eiji; Yamasaki, Kenji; Hiyama, Tamejiro
Synthesis, 1998 , # 10 p. 1544 - 1549
反应条件
1: With water; palladium diacetate; caesium carbonate; sodium thiosulfate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in toluene; tert-butyl alcohol T=80°C; 24 h; Inert atmosphere; 2: With hydrogenchloride; zinc in water 1 h; Cooling with ice;
参考文献
Yi, Jun; Fu, Yao; Xiao, Bin; Cui, Wei-Chen; Guo, Qing-Xiang
Tetrahedron Letters, 2011 , vol. 52, # 2 p. 205 - 208
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] dichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride in N,N-dimethyl-formamide T=100°C; Stille carbonylative cross-coupling; 16 h;
参考文献
Lindh, Jonas; Fardost, Ashkan; Almeida, Maria; Nilsson, Peter
Tetrahedron Letters, 2010 , vol. 51, # 18 p. 2470 - 2472
