water-d2; diisobutylaluminium hydride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride 1) THF, -78 deg C to 0 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuan, Kaixu; Scott, William J.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6188 - 6194
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in diethyl ether Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
Iliceto,A. et al.
Gazzetta Chimica Italiana, 1960 , vol. 90, p. 660 - 670
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Roblin; Davidson; Bogert
Journal of the American Chemical Society, 1935 , vol. 57, p. 151,155
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran T=-78 - 25°C; 24 h; with other catalyst (<1,1'-bis(diphenylphosphino)ferrocene>palladium(0) (dppf)Pd(0)) or without, other solvent, other reaction temperatures; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 55, # 25 p. 6188 - 6194