(R)-苄氧甲基环氧乙烷合成路线 （共 39 条）
反应条件
sodium hydroxide in ethylene glycol dimethyl ether 24 h; Ambient temperature; Yield given;
参考文献
Synthesis, , # 5 p. 503 - 504
反应条件
1: 96 percent / 1,2-dichloro-ethane / 18 h / Heating 2: 94 percent / DIBAL-H / CH2Cl2 / 1 h / -78 °C 3: 98 percent / NaOMe / methanol / 1 h / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 36, # 41 p. 7367 - 7370
反应条件
1: 94 percent / DIBAL-H / CH2Cl2 / 1 h / -78 °C 2: 98 percent / NaOMe / methanol / 1 h / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 36, # 41 p. 7367 - 7370
反应条件
1: NaNO2, H2SO4 / 16 h / Ambient temperature 2: 70 percent / H+ 3: LiAlH4 / tetrahydrofuran 4: pyridine 5: sodium methoxide View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 70 percent / H+ 2: LiAlH4 / tetrahydrofuran 3: pyridine 4: sodium methoxide View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: LiAlH4 / tetrahydrofuran 2: pyridine 3: sodium methoxide View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 40 p. 5505 - 5506
反应条件
1: 94 percent / NBS / CCl4 / 26 h 2: NaOH / 1,2-dimethoxy-ethane / 24 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 5 p. 503 - 504
反应条件
1: 91 percent / acetic anhydride / 1.5 h / Heating 2: 91 percent / K2CO3 / methanol / 0.5 h / 25 °C 3: 61 percent / triphenylphosphine, diethyl azodicarboxylate / benzene / 20 h / Heating View Scheme
参考文献
Synthesis, , # 2 p. 116 - 117
反应条件
1: 91 percent / K2CO3 / methanol / 0.5 h / 25 °C 2: 61 percent / triphenylphosphine, diethyl azodicarboxylate / benzene / 20 h / Heating View Scheme
参考文献
Synthesis, , # 2 p. 116 - 117
反应条件
triphenylphosphine; diethylazodicarboxylate in benzene 20 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 10 p. 1424 - 1424
