2,2,4,4-四甲基-3-戊醇合成路线 (共 29 条)
反应条件
in benzene T=24.75°C;
参考文献
Journal of Organic Chemistry, , vol. 67, # 13 p. 4602 - 4604
反应条件
in diethyl ether; pentane 12 h, from -90 deg C to room temp.;
参考文献
Bestmann, Hans Juergen; Haas, Wolfgang; Witzgall, Konrad; Ricci, Alfredo; Lazzari, Dario; et al.
Liebigs Annalen, 1995 , # 2 p. 415 - 418
反应条件
hydrogenchloride; methanol in toluene Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 8 p. 1472 - 1476
反应条件
diethyl ether T=-40°C;
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 871;engl.Ausg.S.895
Bulletin de la Societe Chimique de France, , p. 178
反应条件
titanium tetrachloride; lithium in tetrahydrofuran T=20°C; McMurry reaction; 24 h; Product distribution; Further Variations:Solvents;
参考文献
Journal of Organometallic Chemistry, , vol. 617-618, p. 744 - 747
参考文献
Acta Chemica Scandinavica, , vol. 53, # 5 p. 352 - 355
反应条件
in diethyl ether T=25°C; 1 h; effects of salts (MeOK, PhCH2OK, (Me2NCH2)2CHOK, MeONa, t-BuOLi, Bu4NBr, BzlEt3NCl); Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3281 - 3286
反应条件
in diethyl ether T=25°C; 1 h; effects of salts (MeOK, t-BuOLi), other reaction time: 24 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3281 - 3286
反应条件
toluene-4-sulfonic acid in benzene 4 h; Heating;
参考文献
Olah, George A.; Wu, An-hsiang; Farooq, Omar; Prakash, G. K. Surya
Journal of Organic Chemistry, 1990 , vol. 55, # 6 p. 1792 - 1796
参考文献
Whitmore; Stahly
Journal of the American Chemical Society, 1933 , vol. 55, p. 4156