5-硝基-2-(3-吡啶基)苯并咪唑合成路线 (共 7 条)
反应条件
[bis(acetoxy)iodo]benzene in ethanol T=20°C;
参考文献
Jung, Myung Hee; Park, Jung Mee; Lee, Ihl-Young Choi; Ahn, Mija
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 1 p. 37 - 44
反应条件
sulfuric acid; nitric acid T=0 - 20°C; Nitration; 2 h;
参考文献
Ambacheu; Pleshakov; Baatkh; Zvolinskii; Kharlamova; Obynochnyi; Prostakov
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 4 p. 421 - 428
反应条件
1: With 4-(N,N-dimethlyamino)pyridine; N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide in N,N-dimethyl-formamide T=25°C; 4 h; 2: With sodium hydroxide in N,N-dimethyl-formamide T=100°C; 10 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 3 p. 695 - 699
反应条件
Na2S2O5 in ethanol 4 h; Reflux;
参考文献
Jain, Priyal; Sharma, Prakash Kumar; Rajak, Harish; Pawar, Rajesh Singh; Patil, Umesh Kumar; Singour, Pradeep Kumar
Archives of Pharmacal Research, 2010 , vol. 33, # 7 p. 971 - 980
反应条件
2: 81.3 percent / conc. nitric acid; conc. sulfuric acid / 2 h / 0 - 20 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 36, # 4 p. 421 - 428
反应条件
2: 81.3 percent / conc. nitric acid; conc. sulfuric acid / 2 h / 0 - 20 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 36, # 4 p. 421 - 428
反应条件
calcium chloride; zinc in ethanol Reduction; 2 h; Heating;
参考文献
Ambacheu; Pleshakov; Baatkh; Zvolinskii; Kharlamova; Obynochnyi; Prostakov
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 4 p. 421 - 428