反应条件
in tetrahydrofuran N2 atmosphere, treatment of THF solns. (2 equiv. H2CPMe3, -78°C), stirring (5 h, warming to 0°C), voltiles removal (0°C); extraction (benzene), filtn. (Celite), recrystn. (toluene); elem. anal.;
参考文献
Cramer, Roger E.; Bruck, Michael A.; Edelmann, Frank; Afzal, Dawood; Gilje, John W.; Schmidbaur, Hubert
Chemische Berichte, 1988 , vol. 121, p. 417 - 420
