2,5-二苯基-1,3,4-噻二唑合成路线 (共 67 条)
反应条件
hydrogenchloride in methanol
1 h; Heatingvarious thitriazepines, hydrolysis; Product distribution;
参考文献
Moss, Stephen F.; Taylor, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 1999 - 2006
反应条件
ethanol; iron(III) chloride
参考文献
Holmberg
Arkiv foer Kemi, 1956 , vol. 9, p. 65,77
反应条件
ethanol; iron(III) chloride
参考文献
Holmberg
Arkiv foer Kemi, 1956 , vol. 9, p. 65,77
反应条件
dihydrogen peroxide; acetone
参考文献
Holmberg
Arkiv foer Kemi, 1956 , vol. 9, p. 65,77
参考文献
Alemagna,A.; Bacchetti,T.
Gazzetta Chimica Italiana, 1972 , vol. 102, p. 1077 - 1083
反应条件
1: 82 percent / ethanol / 1 h / 60 °C
2: 69 percent / 20 h / 240 °C / sealed tube
View Scheme
参考文献
Flowers, William T.; Robinson, John F.; Taylor, David R.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 349 - 355
反应条件
1: 65 percent / 70 percent HClO4, acetic anhydride / 2 h / 60 °C
2: 22 percent / N2H4*H2O (80percent) / Ambient temperature
View Scheme
参考文献
Yonemoto, Katsumi; Shibuya, Isao; Tsuchiya, Tohru; Masahiko Yasumoto; Taguchi, Yoichi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2933 - 2937
反应条件
1: Na2S, sulfur, Py, H2O / Heating
2: (i) aq. HCl, NaNO2, (ii) KH2PO2
View Scheme
参考文献
Krasovitskii,B.M. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2608 - 2613,2589 - 2594
参考文献
Vereshchagina,N.N.; Postovskii,I.Y.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 4024 - 4026,3983 - 3985
参考文献
Huisgen,R. et al.
Chemische Berichte, 1961 , vol. 94, p. 1555 - 1562