2,5-二苯基-1,3,4-噻二唑合成路线 （共 67 条）
反应条件
triethylamine in methanol
参考文献
Glotova, T. E.; Nakhmanovich, A. S.; Komarova, T. N.; Sigalov, M. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 11 p. 2376 - 2377
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 11 p. 2637 - 2638
反应条件
2,4-bis(4-methoxyphenyl)-1,3,4,2-dithiadiphosphetane in toluene
T=110°C; 3 h;
参考文献
El-Barbary, A. A.; Scheibye, S.; Lawesson, S.-O.; Fritz, H.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 597 - 602
参考文献
Glotova, T. E.; Nakhmanovich, A. S.; Sigalov, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # l p. 568 - 571
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 5 p. 680 - 682
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - -55°C; 0.333333 h;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
diphosphorus pentasulfide
T=210°C; im Vakuum;
参考文献
Stolle; Kind
Journal fuer Praktische Chemie (Leipzig), 1904 , vol. <2> 70, p. 428
反应条件
1: 76 percent / Me3Al / benzene; toluene / 6 h / Thermolysis
2: 43 percent / NaH; I2
View Scheme
参考文献
Farrar, John M.; Patel, Mahesh K.; Kaszynski, Piotr; Young Jr., Victor G.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 931 - 940
反应条件
1: sodium hydrosulfide / ethanol / 10 h / Heating
2: hydrazine hydrate / aq. ethanol / 9 h / Heating
3: 65 percent / pyridine / methanol / Heating
View Scheme
参考文献
Poddubnyi; Belen'kii; Krayushkin
Russian Chemical Bulletin, 1996 , vol. 45, # 5 p. 1185 - 1188
反应条件
dihydrogen peroxide in ethanol
0.05 h; Heating; Title compound not separated from byproducts;
参考文献
Kurzer, Frederick; Doyle, Kevin M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1873 - 1880
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - -55°C; 0.333333 h; Title compound not separated from byproducts;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
diphosphorus pentasulfide
T=210°C; im Vakuum;
参考文献
Stolle; Kind
Journal fuer Praktische Chemie (Leipzig), 1904 , vol. <2> 70, p. 428
