2,5-二苯基-1,3,4-噻二唑合成路线 （共 67 条）
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - 20°C;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
sulfur; hydrazine hydrate in ethanol
T=150°C; 1 h; microwave irradiation;
参考文献
Lebrini, Mounim; Bentiss, Fouad; Lagrenee, Michel
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 5 p. 991 - 994
反应条件
sodium hydrogensulfide in ethanol
0.5 h; Heating;
参考文献
Flowers, William T.; Robinson, John F.; Taylor, David R.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 356 - 359
反应条件
disulfur dichloride; triethylamine in dichloromethane
T=0 - 5°C; 2 h;
参考文献
Okuma, Kentaro; Nagakura, Kazuko; Nakajima, Yasutaka; Kubo, Kento; Shioji, Kosei
Synthesis, 2004 , # 12 p. 1929 - 1931
反应条件
thiourea in tetrahydrofuran
T=120 - 150°C;
参考文献
Linganna; Lokanatha Rai
Synthetic Communications, 1998 , vol. 28, # 24 p. 4611 - 4617
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=105°C; 12 h; Inert atmosphere; SolventReagent/catalystTime;
参考文献
Vachhani, Dipak D.; Sharma, Abhishek; Van Der Eycken, Erik
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8768 - 8774
反应条件
disulfur dichloride; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
T=0 - 5°C;
参考文献
Okuma, Kentaro; Nagakura, Kazuko; Nakajima, Yasutaka; Kubo, Kento; Shioji, Kosei
Synthesis, 2004 , # 12 p. 1929 - 1931
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=105°C; 12 h; Inert atmosphere;
参考文献
Vachhani, Dipak D.; Sharma, Abhishek; Van Der Eycken, Erik
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8768 - 8774
反应条件
tert-butylhypochlorite in dichloromethane
T=-70 - -55°C; 0.333333 h;
参考文献
Demchuk, D. V.; Lutsenko, A. I.; Troyanskii, E. I.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.2 p. 1690 - 1695
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1843 - 1848
反应条件
N,N'-di-tert-butylthiourea in ethanol
T=25°C;
参考文献
Moss, Stephen F.; Taylor, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 1981 - 1986
