反应条件
1: NaNO2 / H2O / 0.25 h / -5 - 2 °C 2: 78 percent / CaO, LiCl, CuCl*2H2O / acetone; H2O / 1.) 2 h, 3 to 10 deg C, 2.) 2 h, 10 deg C to room temp., 3.) 2 h, room temp. 3: 68 percent / Fe, HOAc, NaOAc*2H2O / ethanol; H2O / 2 h / Heating View Scheme
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069