N-乙酰氧基-N-丁氧基-4-联苯甲酰胺合成路线 （共 6 条）
反应条件
in acetone Ambient temperature;
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: 20 percent / potassium hydroxide, hydroxylamine hydrochloride / methanol 2: 73 percent / sodium carbonate / methanol; H2O 3: tert-butyl hypochlorite / CH2Cl2 / 3 h 4: 82 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: tert-butyl hypochlorite / CH2Cl2 / 3 h 2: 82 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
1: 73 percent / sodium carbonate / methanol; H2O 2: tert-butyl hypochlorite / CH2Cl2 / 3 h 3: 82 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
反应条件
in methanol-d4
T=34.9°C; Ea, ΔS(excit.); Rate constantThermodynamic data;
参考文献
Campbell, John J.; Glover, Stephen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 10 p. 1661 - 1663
反应条件
in methanol-d4
T=34.85°C; Rearrangement; KineticsActivation energy; Further Variations:Temperatures;
参考文献
Campbell, John J.; Glover, Stephen A.
Journal of Chemical Research, Miniprint, 1999 , # 8 p. 2075 - 2096
