3-甲基丙烯酰氧基丙基甲基二甲氧基硅烷合成路线 (共 2 条)
反应条件
1: ethylene,methyl methacrylate With 2,6-di-tert-butyl-4-(4-methyl-piperazin-1-ylmethyl)-phenol; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex T=80°C; Inert atmosphere; 2: methyl dimethoxy silane With 2,6-di-tert-butyl-4-methyl-phenol T=80°C; Inert atmosphere;
参考文献
Dow Corning Toray Co., Ltd.
Patent: EP2228362 A1, 2010 ;
Location in patent: Page/Page column 13 ;
反应条件
1: 2-methyl-2-propenoic acid With potassium hydroxide in toluene 2: (3-chloropropyl)methyldimethoxysilane With 4,4'-bismethylene(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in toluene; butanone T=110°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1081 - 1092