3-溴三环[4.3.1.13,8]十一烷合成路线 (共 10 条)
反应条件
phosphorus tribromide
参考文献
Molle, Gerard; Bauer, Pierre
Journal of the American Chemical Society, 1982 , vol. 104, # 12 p. 3481 - 3487
反应条件
1: 3.4 percent / diethyl ether / 2.25 h / -20 °C 2: 5.5 g / thionyl bromide / CH2Cl2 / 3 h / Heating View Scheme
参考文献
Molle, Gerard; Bauer, Pierre
Journal of the American Chemical Society, 1982 , vol. 104, # 12 p. 3481 - 3487
反应条件
1: Na2CO3 / bis-(2-methoxy-ethyl) ether; H2O 2: PBr3 View Scheme
参考文献
Nordlander,J.E. et al.
Journal of the American Chemical Society, 1966 , vol. 88, # 19 p. 4475 - 4484
反应条件
phosphorus pentabromide benzene, room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Molle, Gerard; Bauer, Pierre
Journal of the American Chemical Society, 1982 , vol. 104, # 12 p. 3481 - 3487
参考文献
Stepanov,F.N.; Guts,S.S.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 1868 - 1871
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 11 p. 1933 - 1936
反应条件
1: (electrolysis) 2: aq. HBr View Scheme
参考文献
Stepanov,F.N.; Guts,S.S.
Journal of Organic Chemistry USSR (English Translation), 1968 , vol. 4, p. 1868 - 1871
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 11 p. 1933 - 1936
反应条件
1: LiAlH4 2: aq. NaNO2, AcOH 3: PBr3 View Scheme
参考文献
Stetter,H.; Goebel,P.
Chemische Berichte, 1963 , vol. 96, p. 550 - 555
反应条件
1: aq. NaNO2, AcOH 2: PBr3 View Scheme
参考文献
Stetter,H.; Goebel,P.
Chemische Berichte, 1963 , vol. 96, p. 550 - 555
反应条件
(i) H2SO4, (ii) NaOH; Multistep reaction;
参考文献
Stepanov,F.N.; Guts,S.S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , p. 373 - 376
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , # 2 p. 430 - 434
反应条件
formic acid; sulfuric acid
参考文献
Stepanov,F.N.; Guts,S.S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , p. 373 - 376
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , # 2 p. 430 - 434