2-(二甲基氨基)苯磺酸合成路线 (共 11 条)
反应条件
chlorosulfonic acid in 1,2-dichloro-benzene T=50°C; 1 h; E(activ), oth. temperatures; Product distributionKineticsMechanism;
参考文献
Khelevin, R. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 11 p. 2557 - 2565,2276 - 2283
反应条件
sulfuric acid T=60°C; 1 h;
参考文献
Khelevin, R. N.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 1 p. 184 - 189,162 - 166
反应条件
sulfur dioxide T=0°C;
参考文献
Bamberger; Tschirner
Chemische Berichte, 1899 , vol. 32, p. 1883,1893
反应条件
sulfur dioxide; water
参考文献
Bamberger; Tschirner
Chemische Berichte, 1899 , vol. 32, p. 1883,1893
参考文献
Brand; Rutherford
Journal of the Chemical Society, 1952 , p. 3927,3929
参考文献
Grammaticakis
Bulletin de la Societe Chimique de France, 1954 , p. 99,101
反应条件
sulfuric acid T=180°C; other temperatures; other conc. of H2SO4; E(activ.); Rate constantKinetics;
参考文献
Khelevin, R. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 3 p. 603 - 611,531 - 538
反应条件
in 1,2-dichloro-benzene T=180°C; 0.5 h; other temperature (165 and 195 deg C), reaction time 7 h, activation energy; Rate constantThermodynamic dataKinetics;
参考文献
Khelevin, R. N.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 10 p. 1906 - 1911
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 10 p. 2126 - 2131
反应条件
sulfuric acid T=180°C; 7 h; ΔE(act.), various time, various temperature, various excess of H2SO4; Thermodynamic dataKineticsProduct distribution;
参考文献
Khelevin, R. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1723 - 1726
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 9 p. 1889 - 1893
反应条件
phosphoric acid T=180°C; oth. temperatures, E(activ), ΔS(activ.); Rate constantThermodynamic data;
参考文献
Krylov, E. N.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1843 - 1850,1637 - 1644