反应条件
lithium aluminium tetrahydride in tetrahydrofuran
condensing of MeGeCl3 to THF, degassing and cooling (0°C), very slow addn. of LiAlH4; passing through three trap system, collection at -160°C (isopentane slush), fractional distn.;
参考文献
Durig, J. R.; Sullivan, J. F.; Attia, G. M.
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1986 , vol. 42, # 2/3 p. 75 - 88