反应条件
1.1: hexyllithium / tetrahydrofuran; hexane / 1.5 h / 5 - 15 °C 1.2: 62 percent / tetrahydrofuran; hexane / 2 h / 20 °C 2.1: 98.8 percent / H2 / Pd/C / methanol / 24 h / 30 °C / 7500.6 Torr 3.1: 99 percent / PTSA / methanol / 4 h / 40 °C 4.1: 67.4 percent / Bu2SnO; Et3N / CH2Cl2 / 0 - 20 °C 5.1: 99.5 percent / imidazole; Et3N / dimethylformamide / 1.33 h / 0 - 20 °C 6.1: 89 percent / NaI; pyridine / dimethylformamide / 2.5 h / 75 - 80 °C 7.1: 99 percent / LiOH*H2O / methanol; H2O / 8 h View Scheme
参考文献
Martynow, Jacek G.; Jozwik, Julita; Szelejewski, Wieslaw; Achmatowicz, Osman; Kutner, Andrzej; Wisniewski, Krzysztof; Winiarski, Jerzy; Zegrocka-Stendel, Oliwia; Golebiewski, Piotr
European Journal of Organic Chemistry, 2007 , # 4 p. 689 - 703
