反应条件
1: 100 percent / 20 h / 60 °C / 8 Torr / Candida antarctica lipase immobilized on Florisil with Triton X-100 2: 91 percent / pyridine, 4-(N,N-dimethylamino)pyridine / 1 h / 0 °C 3: 100 percent / Na2Cr2O7, H2SO4 / diethyl ether / Ambient temperature 4: 1) aq. NaOH, hydrazine hydrate / 1) diethylene glycol, 100 deg C, 2 h, 2) CH2Cl2, ether 5: 100 percent / 48 h / 60 °C / 8 Torr / Candida antarctica lipase immobilized on Florisil with Triton X-100 6: 95 percent / Na2Cr2O7, H2SO4 / diethyl ether / Ambient temperature 7: 79 percent / NaOH / ethanol; H2O / 3 h / 90 °C View Scheme
参考文献
ERREGIERRE S.P.A.; FERRARI, Massimo; ZINETTI, Fabrizio
Patent: WO2014/20024 A1, 2014 ;
