N-(1-丁基戊基亚基)羟胺合成路线 (共 5 条)
反应条件
hydroxylamine in water; isopropyl alcohol T=110°C; 18.0833 h; Inert atmosphere;
参考文献
Moran, Joseph; Pfeiffer, Jennifer Y.; Gorelsky, Serge I.; Beauchemin, Andre M.
Organic Letters, 2009 , vol. 11, # 9 p. 1895 - 1898
反应条件
hydroxylamine hydrochloride
参考文献
Terent'ev, Alexander O.; Krylov, Igor B.; Ogibin, Yuri N.; Nikishin, Gennady I.
Synthesis, 2006 , # 22 p. 3819 - 3824
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 35°C; Etherification; Alkylation; Hydrolysis; 2.5 h;
参考文献
Tarasova; Shmidt; Sinegovskaya; Petrova; Sobenina; Mikhaleva; Brandsma; Trofimov
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 11 p. 1581 - 1586
反应条件
carbon monoxide; tri-ruthenium(0)dodecacarbonyl in benzene
T=100°C; P=15200 Torr; 8 h;
参考文献
Akazome, Motohiro; Tsuji, Yasushi; Watanabe, Yoshihisa
Chemistry Letters, 1990 , # 4 p. 635 - 638
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in toluene
T=140°C; 4 h;
参考文献
Bayer Intellectual Property GmbH; Gürtler, Christoph; Müller, Thomas Ernst; Gebauer, Ewa; Vogt, Henning; Berezhanskyy, Yevgen; Köhler, Burkhard; Leitner, Walter
Patent: US2013/66112 A1, 2013 ;
Location in patent: Paragraph 0093 ;