2,2-二氯-1-甲基环丙烷羧酸甲酯合成路线 （共 10 条）
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride with different solvents;
参考文献
Fedorynski, Michall
Tetrahedron, 1999 , vol. 55, # 20 p. 6329 - 6334
反应条件
N(Et)4(1+)*(2-pyrrolidone-anion) in N,N-dimethyl-formamide -75 deg C to r.t.;
参考文献
Tetrahedron Letters, , vol. 31, # 49 p. 7181 - 7184
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane Heating;
参考文献
Fedorynski; Blazejczyk; Makosza
Polish Journal of Chemistry, 2003 , vol. 77, # 6 p. 709 - 717
反应条件
1: NaOH; BnNEt3Cl / H2O / 4 h / 20 - 22 °C 2: 15.9 percent / NaOH; BnNEt3Cl / CH2Cl2 / Heating View Scheme
参考文献
Polish Journal of Chemistry, , vol. 77, # 6 p. 709 - 717
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 1 p. 82 - 84
反应条件
1,1-dimethylethylmagnesium chloride; Co(1,2-bis-(diphenylphosphino)ethane)Cl2 Reduction;
参考文献
Wakasugi, Kazunori; Nishii, Yoshinori; Tanabe, Yoo
Tetrahedron Letters, 2000 , vol. 41, # 31 p. 5937 - 5942
反应条件
chiral Ni complex in N,N-dimethyl-formamide Electrochemical reaction; Kinetics;
参考文献
Yanilkin; Strunskaya; Nastapova; Maksimyuk; Bredikhina; Sharafutdinova; Bredikhin
Russian Chemical Bulletin, 2003 , vol. 52, # 4 p. 923 - 928
反应条件
2,2'-azo-bisisobutyronitrile; (S-i-pr)3SiH in toluene T=75 - 90°C; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 8 p. 2427 - 2433
反应条件
1: 91 percent / LiAlH4 / tetrahydrofuran / 5 h / Ambient temperature
2: 89 percent / PCC / CH2Cl2 / 20 h / Ambient temperature
View Scheme
参考文献
Tanabe, Yoo; Seko, Shinzo; Nishii, Yoshinori; Yoshida, Taichi; Utsumi, Naoka; Suzukamo, Gohfu
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 17 p. 2157 - 2165
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
5 h; Ambient temperature;
参考文献
Tanabe, Yoo; Seko, Shinzo; Nishii, Yoshinori; Yoshida, Taichi; Utsumi, Naoka; Suzukamo, Gohfu
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 17 p. 2157 - 2165
