1-溴-5-(4-甲氧苯基)戊烷合成路线 (共 6 条)
反应条件
phosphorus tribromide; Petroleum ether
参考文献
Moore, J. S.; Stupp, S. I.
Journal of the American Chemical Society, 1992 , vol. 114, # 9 p. 3429 - 3441
反应条件
1: LiAlH4 2: triphenylphosphine, carbon tetrabromide View Scheme
参考文献
van der Zanden
Recueil des Travaux Chimiques des Pays-Bas, 1941 , vol. 60, p. 291,295
反应条件
dilithium tetrachlorocuprate in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Kadkhodayan, Miryam; Singleton, Terry; Heldrich, F. J.
Synthetic Communications, 1984 , vol. 14, # 8 p. 707 - 712
反应条件
1: ethanol; amalgamated zinc; aqueous hydrochloric acid 2: ethanol; sulfuric acid 3: sodium; petroleum ether; ethanol 4: petroleum ether; PBr3 View Scheme
参考文献
van der Zanden
Recueil des Travaux Chimiques des Pays-Bas, 1941 , vol. 60, p. 291,295
反应条件
1: (i) , (ii) (heating), Al2O3 2: (i) B2H6, (ii) (heating), (iii) aq. H2O2, aq. NaOH 3: PBr3 View Scheme
参考文献
Hubert,A.J.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 235 - 238
反应条件
1: (i) B2H6, (ii) (heating), (iii) aq. H2O2, aq. NaOH 2: PBr3 View Scheme
参考文献
Hubert,A.J.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 235 - 238