2-(三氟甲基)苯并噻唑合成路线 (共 13 条)
反应条件
palladium dichloride in dimethyl sulfoxide
T=110°C; 3 h;
参考文献
Zhu, Jiangtao; Chen, Zixian; Xie, Haibo; Li, Shan; Wu, Yongming
Organic Letters, 2010 , vol. 12, # 10 p. 2434 - 2436
参考文献
Rene, Olivier; Souverneva, Alexandra; Magnuson, Steven R.; Fauber, Benjamin P.
Tetrahedron Letters, 2013 , vol. 54, # 3 p. 201 - 204
反应条件
copper(l) iodide; sodium hydrogen sulfide hydrate; H2O4P(1-)*3K(1+) in N,N-dimethyl-formamide
T=80°C; Ullmann reaction; 10 h;
参考文献
Li, Chun-Lin; Zhang, Xing-Guo; Tang, Ri-Yuan; Zhong, Ping; Li, Jin-Heng
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 7037 - 7040
反应条件
1,10-phenanthroline; di-tert-butyl peroxide; copper diacetate; sodium acetate; sodium t-butanolate in 1,2-dichloro-ethane
T=80°C; 6.03333 h; Inert atmosphereMolecular sieve;
参考文献
Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 2 p. 1298 - 1304
反应条件
acetic acid
T=120°C; Cyclization; Condensation; 8 h;
参考文献
Wang, Quan-Fu; Mao, Yun-Yu; Zhu, Shi-Zheng; Hu, Chang-Ming
Journal of Fluorine Chemistry, 1999 , vol. 95, # 1-2 p. 141 - 143
参考文献
Alvernhe, Gerard M.; Laurent, Andre J.; Drean, Isabelle M. Le; Selmi, Abdelaziz
Tetrahedron Letters, 1993 , vol. 34, # 15 p. 2483 - 2486
Title/Abstract Full Text View citing articles Show Details
Alvernhe, Gerard; Greif, Dieter; Langlois, Bernard; Laurent, Andre; Drean, Isabelle Le; et al.
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 167 - 172
反应条件
1: sodium hydrosulfide monohydrate / ethanol / 20 °C
2: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / acetonitrile / 0.5 h / 80 °C
View Scheme
参考文献
Zhu, Jiangtao; Xie, Haibo; Li, Shan; Chen, Zixian; Wu, Yongming
Journal of Fluorine Chemistry, 2011 , vol. 132, # 5 p. 306 - 309
反应条件
2-amino-benzenethiol in ethanol
Ambient temperature;
参考文献
Alyea, Elmer C.; Malek, Abdul
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1325 - 1327
参考文献
Alvernhe, Gerard; Greif, Dieter; Langlois, Bernard; Laurent, Andre; Drean, Isabelle Le; et al.
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 167 - 172
反应条件
in dimethyl sulfoxide
Heating;
参考文献
Alyea, Elmer C.; Malek, Abdul
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1325 - 1327