(S)-(+)-2-叔-丁基氨基-1-苯基乙醇合成路线 （共 14 条）
反应条件
ytterbium(III) triflate in dichloromethane 1 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 3 p. 433 - 436
反应条件
in ethanol T=195°C; P=12929 Torr; 0.0833333 h; Product distribution / selectivity;
参考文献
US2011/118469 A1, ;
Page/Page column 9-10 ;
反应条件
sodium tetrahydroborate in tetrahydrofuran; ethanol 0.5 h;
参考文献
Ayala-Mata, Francisco; Barrera-Mendoza, Citlalli; Jimenez-Vazquez, Hugo A.; Vargas-Diaz, Elena; Zepeda, L. Gerardo
Molecules, 2012 , vol. 17, # 12 p. 13864 - 13878
反应条件
in 2,2,2-trifluoroethanol T=20°C; 6 h; regioselective reaction;
参考文献
Khaksar, Samad; Heydari, Akbar; Tajbakhsh, Mahmood; Bijanzadeh, Hamid Reza
Journal of Fluorine Chemistry, 2010 , vol. 131, # 1 p. 106 - 110
反应条件
sodium tetrahydroborate in methanol 0.5 h; Ambient temperature;
参考文献
Alcaide, Benito; Escobar, Gerardo; Perez-Ossorio, Rafael; Plumet, Joaquin; Sanz, Dionisia
Journal of Chemical Research, Miniprint, 1984 , # 5 p. 1466 - 1488
反应条件
1: in tetrahydrofuran T=20°C; 20 h; 2: With sodium sulfite in tetrahydrofuran Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 10 p. 2243 - 2252
反应条件
Cr(NtBu)2Cl2 in dichloromethane 240 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 1 p. 107 - 108
反应条件
in ethanol T=195°C; P=12929 Torr; 0.0833333 h;
参考文献
Organic Process Research and Development, , vol. 14, # 2 p. 432 - 440
反应条件
1.1: sodium tetrahydroborate / ethanol / 0.5 h 1.2: 0.25 h 2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.5 h View Scheme
参考文献
Molecules, , vol. 17, # 12 p. 13864 - 13878
反应条件
(i) Py, Et2O, (ii) LiAlH4; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 97, p. 2305 - 2307
