boron trifluoride diethyl etherate in dichloromethane a) -30 deg C, 1h, b) 10 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Moiseenkov, A. M.; Veselovskii, V. V.; Dragan, V. A.; Ignatenko, A. V.; Strelenko, Yu. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 6 p. 1233 - 1237
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 6 p. 1368 - 1372
boron trifluoride diethyl etherate in dichloromethane T=-30°C;
参考文献
Dragan, V. A.; Veselovskii, V. V.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.2 p. 210
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 227 - 228
lithium aluminium tetrahydride in tetrahydrofuran
17 h; RefluxInert atmosphere;
参考文献
Xuan, Mengyang; Paterson, Ian; Dalby, Stephen M.
Organic Letters, 2012 , vol. 14, # 21 p. 5492 - 5495,4
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Xuan, Mengyang; Paterson, Ian; Dalby, Stephen M.
Organic Letters, 2012 , vol. 14, # 21 p. 5492 - 5495
{CpRu[P(i-Pr)2(1-Me-4-tBu-imidazol-2-yl)]MeCN}*PF6 in acetone
T=25°C; 96 h;
参考文献
Grotjahn, Douglas B.; Larsen, Casey R.; Gustafson, Jeffery L.; Nair, Reji; Sharma, Abhinandini
Journal of the American Chemical Society, 2007 , vol. 129, # 31 p. 9592 - 9593
dibenzo-18-crown-6; ammonia; sodium in tetrahydrofuran
T=-70°C;
参考文献
Moiseenkov, A. M.; Ishchenko, R. I.; Veselovskii, V. V.; Odinokov, V. N.; Polunin, E. V.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 366 - 368
Khimiya Prirodnykh Soedinenii, 1989 , # 3 p. 422 - 424