反应条件
1: tri-n-butyl-tin hydride; 2,2'-azo-bisisobutyronitrile / toluene / 16 h / 130 °C / |Inert atmosphere
2: benzotriazol-1-ol; dicyclohexyl-carbodiimide; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 16 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Abe, Takumi; Nakamura, Shuuhei; Yanada, Reiko; Choshi, Tominari; Hibino, Satoshi; Ishikura, Minoru
Organic Letters, 2013 , vol. 15, # 14 p. 3622 - 3625