反应条件
1: 30 percent / NaH / tetrahydrofuran / 60 °C 2: 89 percent / H2, 5N HCl / Pd-C / methanol; H2O 3: 1) DIBAL-H, 2) (COCl)2, DMSO, Et3N / 1) toluene, -35 deg C -> 25 deg C, 2) CH2Cl2, -70 deg C View Scheme
参考文献
Sternfeld, Francine; Baker, Raymond; Broughton, Howard B.; Guiblin, Alexander R.; Jelley, Richard A.; Matassa, Victor G.; Reeve, Austin J.; Beer, Margaret S.; Stanton, Josephine A.; Hargreaves, Richard J.; Shepheard, Sara L.; Longmore, Jeanette; Razzaque, Zerin; Graham, Michael I.; Sohal, Bindi; Street, Leslie J.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 15 p. 1825 - 1830
