反应条件
in tetrahydrofuran addn. of equimolar amount of cyclopropene to soln. of K salt in THF at ambient temp. under N2; stirring for 15 min;; evapn. to dryness; addn. of toluene; filtration; concn.; chromy. (silica, -10°C, toluene: isolation of Cr arenes, then ether); concn.; dissolving in toluene and addn. of petroleum ether; storage at - 78°C; pptn.; elem. anal.;;
参考文献
Schubert, Juergen; Mock, Stefan; Schubert, Ulrich
Chemische Berichte, 1993 , vol. 126, # 3 p. 657 - 664