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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1440510-01-9
合成路线
(共 5 条)
1440510-01-9
→
反应条件
303963-92-0
(3Ar,6ar)-6-((叔丁基二苯基甲硅烷基氧基)甲基)-2,2-二甲基-3ah-环戊并[d][1,3]二氧代l-4(6ah)-酮
反应条件
dipyridinium dichromate in N,N-dimethyl-formamide T=20°C; 12 h; Molecular sieve;
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng
MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826
67814-68-0
→
反应条件
1440510-01-9
反应条件
<b>Multi-step reaction with 5 steps<br /> </b>1: triethylamine; dmap / N,N-dimethyl-formamide<br />2: potassium <i>tert</i>-butylate / tetrahydrofuran<br />3: triethylamine; sulfur trioxide pyridine complex / dichloromethane<br />4: tetrahydrofuran / -78 °C<br />5: Grubb's 2nd generation catalyst / dichloromethane / |Reflux<br /> <br />
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826
681853-95-2
→
反应条件
1440510-01-9
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: tetrahydrofuran / -78 °C<br />2: Grubb's 2nd generation catalyst / dichloromethane / |Reflux<br /> <br />
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826
532-20-7
→
反应条件
1440510-01-9
反应条件
<b>Multi-step reaction with 6 steps<br /> </b>1: sulfuric acid<br />2: triethylamine; dmap / N,N-dimethyl-formamide<br />3: potassium <i>tert</i>-butylate / tetrahydrofuran<br />4: triethylamine; sulfur trioxide pyridine complex / dichloromethane<br />5: tetrahydrofuran / -78 °C<br />6: Grubb's 2nd generation catalyst / dichloromethane / |Reflux<br /> <br />
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826
681853-93-0
→
反应条件
1440510-01-9
反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: triethylamine; sulfur trioxide pyridine complex / dichloromethane<br />2: tetrahydrofuran / -78 °C<br />3: Grubb's 2nd generation catalyst / dichloromethane / |Reflux<br /> <br />
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826