2-氯-1-哌啶-1-基乙酮合成路线 （共 18 条）
参考文献
Li, Yang; Zhang, Yu; Huang, Zhi; Cao, Xiaoping; Gao, Kun
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 622 - 630
参考文献
Korea Research Institute of Chemical Technology
Patent: US6310246 B1, 2001 ;
反应条件
S4N4*SbCl5 in toluene Heating;
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
dicyclohexyl-carbodiimide in diethyl ether T=0 - 20°C;
参考文献
Australian Journal of Chemistry, , vol. 39, # 4 p. 687 - 698
反应条件
in dichloromethane T=-25 - 20°C; 3.5 h;
参考文献
Chemistry of Natural Compounds, , vol. 48, # 6 p. 1047 - 1053
Khim. Prir. Soedin., , vol. 48, # 6 p. 924 - 929,6
反应条件
1.1: KOH / methanol / 0.17 h / 0 °C 1.2: 85 percent / methanol / 1 h / 0 °C 2.1: 92 percent / oxone / methanol; H2O / 0 °C 3.1: 82 percent / KOH; Al2O3; CBr2F2 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Li, Yang; Zhang, Yu; Huang, Zhi; Cao, Xiaoping; Gao, Kun
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 622 - 630
反应条件
1: 52 percent / NaH / tetrahydrofuran / 2 h / 20 °C 2: 51 percent / KOH / ethanol / 12 h / 0 °C 3: 28 percent / 0.25 h / 150 °C / 4 Torr 4: 60 percent / LiAlH4 / diethyl ether / 1 h / 0 - 20 °C View Scheme
参考文献
Seguin, Helene; Gardette, Daniel; Moreau, Marie-France; Madelmont, Jean-Claude; Gramain, Jean-Claude
Synthetic Communications, 1998 , vol. 28, # 22 p. 4257 - 4272
参考文献
Landi-Vittory; Marini-Bettolo
Rend.Ist.super.Sanita, 1956 , vol. 19, p. 109,113,115
参考文献
Am.Home Prod.Corp.
Patent: US2654754 , 1950 ;
参考文献
Speziale; Hamm
Journal of the American Chemical Society, 1956 , vol. 78, p. 5580,5582
