N,N’-二羟基-2,3-二甲基-2,3-丁二胺合成路线 （共 16 条）
反应条件
aluminum amalgam in tetrahydrofuran; water T=-7 - -2°C; 0.75 h;
参考文献
Rajca, Andrzej; Pink, Maren; Mukherjee, Sumit; Rajca, Suchada; Das, Kausik
Tetrahedron, 2007 , vol. 63, # 44 p. 10731 - 10742
反应条件
in ethanol 15 h; Heating;
参考文献
Schmidt, Juergen; Zinner, Gerwalt
Archiv der Pharmazie (Weinheim, Germany), 1980 , vol. 313, # 2 p. 174 - 179
反应条件
1: 43 percent / methanol / 16 h / 20 °C 2: 84 percent / lead dioxide / methanol / 0.33 h / 20 °C View Scheme
参考文献
Wu, Yihui; Bi, Lanrong; Bi, Wei; Li, Zeng; Zhao, Ming; Wang, Chao; Ju, Jingfang; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5711 - 5720
反应条件
tert-butylhypochlorite in dichloromethane T=20°C; 2 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 2 p. 330 - 339
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 364 - 375
反应条件
air T=20 - 25°C; 168 h;
参考文献
Shustov, G. V.; Tavakalyan, N. B.; Shustova, L. L.; Pleshkova, A. P.; Kostyanovskii, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 330 - 339
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 364 - 375
反应条件
tert-butylhypochlorite in dichloromethane T=20°C; 2 h;
参考文献
Shustov, G. V.; Tavakalyan, N. B.; Shustova, L. L.; Pleshkova, A. P.; Kostyanovskii, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 2 p. 330 - 339
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 2 p. 364 - 375
反应条件
1: 96 percent / p-TsOH*H2O / methanol / 48 h / 20 °C 2: 85 percent / NaIO4 / CHCl3; H2O / 0 - 20 °C View Scheme
参考文献
Wu, Yihui; Bi, Lanrong; Bi, Wei; Li, Zeng; Zhao, Ming; Wang, Chao; Ju, Jingfang; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 16 p. 5711 - 5720
反应条件
toluene-4-sulfonic acid in methanol
T=20°C; 48 h;
参考文献
Rajca, Andrzej; Pink, Maren; Mukherjee, Sumit; Rajca, Suchada; Das, Kausik
Tetrahedron, 2007 , vol. 63, # 44 p. 10731 - 10742
反应条件
1: 83 percent / ethanol / 0.17 h / Heating
2: 81 percent / NaBH4 / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Schmidt, Juergen; Zinner, Gerwalt
Archiv der Pharmazie (Weinheim, Germany), 1980 , vol. 313, # 2 p. 174 - 179
反应条件
in methanol
T=20°C; 16 h;
参考文献
Zhao, Ming; Li, Zheng; Peng, Li; Tang, Yu-Rong; Wang, Chao; Zhang, Ziding; Peng, Shiqi
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 8 p. 2815 - 2826
