1-氯-4-[(2-氯乙基)硫代]苯合成路线 (共 12 条)
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Gist-Brocades N.V.
Patent: US4496720 A1, 1985 ;
反应条件
thionyl chloride in chloroform 1 h;
参考文献
Angamuthu, Raja; Kooijman, Huub; Lutz, Martin; Spek, Anthony L.; Bouwman, Elisabeth
Dalton Transactions, 2007 , # 41 p. 4641 - 4643
反应条件
aluminium trichloride; nitromethane in carbon disulfide 40 h; Ambient temperature;
参考文献
El-Khawaga, A. M.; El-Zohry, M. F.; Ismail, M. T.; Abdel-Wahab, A. A.; Khalaf, A. A.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 29, p. 265 - 270
参考文献
Schmid,G.H.; Garratt,D.G.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 2463 - 2468
反应条件
magnesium in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Bauld, Nathan L.; Aplin, J. Todd; Yueh, Wang; Endo, Stephanie; Loving, Angie
Journal of Physical Organic Chemistry, 1998 , vol. 11, # 1 p. 15 - 24
反应条件
1: aqueous KOH / 100 °C 2: PCl5 View Scheme
参考文献
Baddeley; Bennett
Journal of the Chemical Society, 1933 , p. 46
反应条件
magnesium in tetrahydrofuran 1 h; Heating;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 13, p. 165 - 168
反应条件
dihydrogen peroxide in acetic acid
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.; Khalaf, Ali A.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 31 - 44
反应条件
1: dihydrogen peroxide; acetic acid 2: sodium hydroxide / methanol View Scheme
参考文献
Padmavathi, Venkatapuram; Venkatesh, Bhumireddy Chinnachennaiahgari; Premakumari, Chokkappagari; Padmaja, Adivireddy
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 3 p. 646 - 651
反应条件
aluminium trichloride in carbon disulfide
3 h; Heating;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; El-Zohry, Maher F.; Khalaf, Ali A.
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 31 - 44