17beta-雌二醇17-(2,3,4-三-O-乙酰基-beta-D-葡糖苷酸甲酯)合成路线 （共 5 条）
反应条件
sodium tetrahydroborate; palladium dichloride in methanol T=0°C; 2 h;
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
反应条件
silver carbonate; benzene
参考文献
Wotiz et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 1704,1706
反应条件
1: 72 percent / Ag2CO3 / benzene / 48 h / Ambient temperature 2: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C View Scheme
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
反应条件
1: 72 percent / Ag2CO3 / benzene / 48 h / Ambient temperature 2: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C View Scheme
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
反应条件
sodium hydroxide in methanol Ambient temperature;
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
