hydrogen; palladium on activated charcoal in N,N-dimethyl-formamide P=2585.7 Torr; 3 h;

1: 93 percent / H2 / 10 percent Pd/C / dimethylformamide / 3 h / 2585.7 Torr 2: 85 percent / LiOH / H2O; methanol / 17 h / 0 °C View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209264', constants.ctx, '0')">hydrogen azide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '610776', constants.ctx, '0')">triphenylphosphine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '908662', constants.ctx, '0')">diethylazodicarboxylate</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '969212', constants.ctx, '0')">benzene</a> <br />3&nbsp;h;&nbsp;&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;