(R)-4-苄氧甲基-2,2-二甲基-1,3-二氧戊环合成路线 （共 11 条）
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride in N,N-dimethyl-formamide
参考文献
Lin, Hong-Jyune; Adak, Avijit Kumar; Reddy, L. Vijaya Raghava; Wu, Shih-Hsiung; Lin, Chun-Cheng
Chemistry - A European Journal, 2013 , vol. 19, # 24 p. 7989 - 7998
反应条件
sodium hydride in tetrahydrofuran 12 h; Ambient temperature;
参考文献
Xia, Jie; Hui, Yong-Zheng
Tetrahedron Asymmetry, 1997 , vol. 8, # 18 p. 3019 - 3021
反应条件
1: 3-benzyloxypropyleneoxide With polymer-supported Co(III)-(R,R)-salen ligand; water T=20°C; 4 h; 2: 2,2-dimethoxy-propane With toluene-4-sulfonic acid Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 8 p. 1309 - 1312
反应条件
1: 79 percent / DIBALH / diethyl ether / 0 °C 2: tetra-n-butylammonium hydrogen sulfate; sodium hydroxide / benzene / 45 °C View Scheme
参考文献
Organic letters, , vol. 4, # 16 p. 2625 - 2628
反应条件
1: 2,2-dimethyl-1,3-dioxolane-4-methanol With sodium hydride in N,N-dimethyl-formamide; mineral oil 0.666667 h; Cooling with ice; 2: benzyl bromide in N,N-dimethyl-formamide; mineral oil T=20°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 20 p. 4311 - 4318
反应条件
1.1: lithium hydroxide hydrate / tetrahydrofuran; water / 12 h / 20 °C 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / |Cooling with ice 2.2: 2 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 20 p. 4311 - 4318
反应条件
1.1: lithium hydroxide hydrate / tetrahydrofuran; water / 12 h / 20 °C 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / |Cooling with ice 2.2: 2 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 20 p. 4311 - 4318
反应条件
1.1: lithium hydroxide hydrate / tetrahydrofuran; water / 12 h / 20 °C 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / |Cooling with ice 2.2: 2 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 20 p. 4311 - 4318
反应条件
tin(ll) chloride 21 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 23 p. 9144 - 9147
参考文献
Tetrahedron Letters, , vol. 29, # 10 p. 1157 - 1160
