(R)-(-)-甘油醇缩丙酮合成路线 （共 67 条）
反应条件
sodium periodate; sodium borohydride; sodium chloride in water; acetone
参考文献
Barrett, Stephen Douglas; Kaufman, Michael David; Rewcastle, Gordon William; Spicer, Julie Ann
Patent: US2003/232889 A1, 2003 ;
Location in patent: Page/Page column 13 ;
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h; Ambient temperature;
参考文献
Wilde, H. De; Clercq, P. De; Vandewalle, M.; Roeper, H.
Tetrahedron Letters, 1987 , vol. 28, # 40 p. 4757 - 4758
参考文献
Tetrahedron Asymmetry, , vol. 5, # 1 p. 5 - 8
Tetrahedron Asymmetry, , vol. 8, # 6 p. 923 - 933
反应条件
sodium tetrahydroborate in ethanol
参考文献
Marco, Jose L.; Rodriguez, Benjamin
Tetrahedron Letters, 1988 , vol. 29, # 16 p. 1997 - 1998
反应条件
sodium hydroxide in methanol; water T=25°C; 30 h;
参考文献
Aragozzini, Fabrizio; Maconi, Elisabetta; Potenza, Donatella; Scolastico, Carlo
Synthesis, 1989 , # 3 p. 225 - 227
反应条件
phosphate buffer; porcine pancreas T=28°C; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 7200
反应条件
sodium hydroxide in ethanol 0.5 h; Heating;
参考文献
D'Arrigo, Paola; Feliciotti, Luca; Pedrocchi-Fantoni, Giuseppe; Servi, Stefano
Journal of Organic Chemistry, 1997 , vol. 62, # 18 p. 6394 - 6396
反应条件
potassium carbonate in methanol 5 h; Ambient temperature;
参考文献
Suemune; Mizuhara; Akita; Sakai
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 8 p. 3440 - 3444
反应条件
1: LiAlH4 / tetrahydrofuran / 2 h / Heating 2: aq. NaIO4 / tetrahydrofuran / 2 h / 0 °C 3: NaBH4 / ethyl acetate; ethanol / 2.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 5 p. 1181 - 1190
反应条件
methanol in di-isopropyl ether T=0°C; 83 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 6 p. 923 - 933
