4-苯基环己基-1-烯-1-羧酸合成路线 （共 10 条）
反应条件
potassium acetate; [Pd(PPh3)2(OAc)2] in N,N-dimethyl-formamide T=25°C; 5 h;
参考文献
Cacchi, Sandro; Lupi, Alessandro
Tetrahedron Letters, 1992 , vol. 33, # 27 p. 3939 - 3942
反应条件
1: With [2,2']bipyridinyl; manganese; NiBr2bipy; tetraethylammonium iodide in 1,3-dimethyl-imidazolidin-2-one T=20°C; P=760.051 Torr; 20 h; 2: With hydrogenchloride; water in diethyl ether T=20°C; 0.166667 h;
参考文献
Fujihara, Tetsuaki; Nogi, Keisuke; Xu, Tinghua; Terao, Jun; Tsuji, Yasushi
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9106 - 9109
反应条件
1: With lithium hydroxide monohydrate; N-benzyl-N,N,N-triethylammonium chloride; water in tert-butyl alcohol T=20°C; 24 h; 2: With hydrogenchloride in water pH=1;
参考文献
Vitnik; Ivanovic; Orevic; Zizak; Juranic
Synthetic Communications, 2009 , vol. 39, # 8 p. 1457 - 1471
反应条件
bis-triphenylphosphine-palladium(II) chloride; tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=20°C; P=760 Torr; electrolyses, carbon cathode, Mg anode, E=-2.0 V;
参考文献
Jutand, Anny; Negri, Serge
European Journal of Organic Chemistry, 1998 , # 9 p. 1811 - 1821
反应条件
1.1: phosphorus pentachloride / dichloromethane; cyclohexane / 1 h / Inert atmosphere; Reflux 2.1: [2,2']bipyridinyl; manganese; NiBr2bipy; tetraethylammonium iodide / 1,3-dimethyl-imidazolidin-2-one / 20 h / 20 °C / 760.05 Torr 2.2: 0.17 h / 20 °C View Scheme
参考文献
Fujihara, Tetsuaki; Nogi, Keisuke; Xu, Tinghua; Terao, Jun; Tsuji, Yasushi
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9106 - 9109
反应条件
1: alcoholic potash / 150 °C / im Autoklaven 2: sodium 3: permanganate 4: water View Scheme
参考文献
Rassow
Justus Liebigs Annalen der Chemie, 1894 , vol. 282, p. 143
反应条件
1: sodium 2: permanganate 3: water View Scheme
参考文献
Rassow
Justus Liebigs Annalen der Chemie, 1894 , vol. 282, p. 143
反应条件
1: permanganate 2: water View Scheme
参考文献
Rassow
Justus Liebigs Annalen der Chemie, 1894 , vol. 282, p. 143
参考文献
Rassow
Justus Liebigs Annalen der Chemie, 1894 , vol. 282, p. 143
反应条件
1: 35 percent / H2SO4 / Heating
2: BH3*Me2S / tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Leopoldo, Marcello; Lacivita, Enza; Colabufo, Nicola A.; Contino, Marialessandra; Berardi, Francesco; Perrone, Roberto
Journal of Medicinal Chemistry, 2005 , vol. 48, # 25 p. 7919 - 7922
