N-甲基-3-甲氧基苯胺合成路线 (共 31 条)
反应条件
1: With sodium methylate in methanol T=20°C; 5 h; 2: With sodium tetrahydroborate in methanol 1.75 h; Heating;
参考文献
Kamino, Shinichiro; Murakami, Miho; Tanioka, Masaru; Shirasaki, Yoshinao; Watanabe, Keiko; Horigome, Jun; Ooyama, Yousuke; Enomoto, Shuichi
Organic Letters, 2014 , vol. 16, # 1 p. 258 - 261
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Tetrahedron, , vol. 27, p. 1253 - 1259
反应条件
triethylsilane; tin(IV) chloride in dichloromethane T=0 - 5°C; Rearrangement; Reduction;
参考文献
Lopez, Francisco J.; Nitzan, Dov
Tetrahedron Letters, 1999 , vol. 40, # 11 p. 2071 - 2074
反应条件
CuCN in tetrahydrofuran T=-50 - 20°C; Arylation; 2 h;
参考文献
Bernardi, Paolo; Dembech, Pasquale; Fabbri, Gaia; Ricci, Alfredo; Seconi, Giancarlo
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 641 - 643
反应条件
1: With trifluoroacetic acid 25 h; Reflux; 2: With sodium tetrahydroborate in ethanol T=20°C; 24 h;
参考文献
Lin, Yu-Chen; Chen, Chao-Tsen
Chemistry - A European Journal, 2013 , vol. 19, # 7 p. 2531 - 2538
反应条件
1: 72 percent / conc. H2SO4 2: 80 percent / 10percent hydrochloric acid / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 17, # 2 p. 225 - 229
反应条件
sodium tetrahydroborate in tetrahydrofuran T=20°C; 12 h;
参考文献
Chinese Chemical Letters, , vol. 21, # 8 p. 939 - 942
反应条件
hydrogenchloride 1 h; Heating;
参考文献
Knierzinger; Wolfbeis
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 2 p. 225 - 229
反应条件
sodium amide; methylamine
参考文献
Journal of Organic Chemistry, , vol. 48, # 23 p. 4397 - 4399
反应条件
water in 1,4-dioxane T=25°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 103, # 23 p. 6908 - 6911