(2-疏基-1-甲基-1H-咪唑-5-基)甲醇合成路线 （共 7 条）
反应条件
in acetic acid; butan-1-ol 72 h; ultrasonic bath;
参考文献
Collman, James P.; Zhong, Min; Costanzo, Simona; Zhang, Chi
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8252 - 8256
反应条件
acetic acid in butan-1-ol 70 h;
参考文献
US2004/9983 A1, ;
Page/Page column 117 ;
反应条件
acetic acid in butan-1-ol 50 h; Ambient temperature;
参考文献
Aulaskari, Paula; Ahlgren, Markku; Rouvinen, Juha; Vainiotalo, Pirjo; Pohjala, Esko; Vepsaelaeinen, Jouko
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1345 - 1354
反应条件
hydrogen in ethanol Reflux;
参考文献
Sarkarzadeh, Hasti; Miri, Ramin; Firuzi, Omidreza; Amini, Mohsen; Razzaghi-Asl, Nima; Edraki, Najmeh; Shafiee, Abbas
Archives of Pharmacal Research, 2013 , vol. 36, # 4 p. 436 - 447
反应条件
1: 71 percent / NaNO2; aq. HNO3 / 0.75 h 2: 95 percent / MnO2 / CHCl3 / 12 h / Heating View Scheme
参考文献
Collman, James P.; Zhong, Min; Costanzo, Simona; Zhang, Chi
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8252 - 8256
反应条件
1: 75 percent / aq. HNO3; NaNO2 / 20 °C 2: 71 percent / MnO2 / CHCl3 / 48 h / Heating 3: methanol; H2O / 20 °C 4: 16.3 g / NaBH4 / methanol; H2O View Scheme
参考文献
Collman, James P.; Zhong, Min; Costanzo, Simona; Zhang, Chi
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8252 - 8256
反应条件
1.1: 85 percent / Raney nickel / ethanol / 3 h / Heating
2.1: SOCl2 / CHCl3 / 1 h / Heating
2.2: HNO3; H2SO4; water / 2 h / 20 °C
2.3: 60 percent / water / propan-2-ol / 24 h / Heating
3.1: 80 percent / MnO2 / CHCl3 / 0.5 h / Heating
View Scheme
参考文献
Shafiee, Abbas; Rastkary, Noushin; Jorjani, Masoumeh; Shafaghi, Bijan
Archiv der Pharmazie (Weinheim, Germany), 2002 , vol. 335, # 2 p. 69 - 76
