N-苯甲基-4-硝基苯胺合成路线 （共 42 条）
反应条件
1: 87 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Ambient temperature 2: 17 percent / t-BuOK / dimethylsulfoxide / 0.25 h / Ambient temperature View Scheme
参考文献
Katritzky, Alan R.; Laurenzo, Kathleen S.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 3978 - 3982
反应条件
1: 87 percent / conc. H2SO4 / ethanol / 4 h / Heating 2: 87 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Ambient temperature 3: 17 percent / t-BuOK / dimethylsulfoxide / 0.25 h / Ambient temperature View Scheme
参考文献
Katritzky, Alan R.; Laurenzo, Kathleen S.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 3978 - 3982
反应条件
in acetonitrile 24 h; Heating;
参考文献
Kotsuki; Kobayashi; Suenaga; Nishizawa
Synthesis, 1990 , # 12 p. 1145 - 1147
反应条件
1,4-diaza-bicyclo[2.2.2]octane in toluene T=150 - 170°C; 1 h; Microwave irradiation;
参考文献
Gonzalez-Arellano, Camino; Yoshida, Kenta; Luque, Rafael; Gai, Pratibha L.
Green Chemistry, 2010 , vol. 12, # 7 p. 1281 - 1287
反应条件
hydrogen in N,N-dimethyl-formamide T=60°C; 0.5 h;
参考文献
Srivani; Prasad, P. S. Sai; Lingaiah
Catalysis Letters, 2012 , vol. 142, # 3 p. 389 - 396
反应条件
1: NEt3 / CH2Cl2 / 0.17 h / -15 °C 2: 61 percent / acetonitrile / 24 h / Heating View Scheme
参考文献
Kotsuki; Kobayashi; Suenaga; Nishizawa
Synthesis, 1990 , # 12 p. 1145 - 1147
反应条件
1: potassium tert-butylate / tetrahydrofuran / 1 h / |Reflux 2: trifluorormethanesulfonic acid / chloroform / 1 h / |Reflux View Scheme
参考文献
King, Frank D.; Caddick, Stephen
Tetrahedron, 2013 , vol. 69, # 40 p. 8592 - 8601
反应条件
1: potassium tert-butylate / tetrahydrofuran / 1 h / |Reflux 2: trifluorormethanesulfonic acid / chloroform / 1 h / |Reflux View Scheme
参考文献
King, Frank D.; Caddick, Stephen
Tetrahedron, 2013 , vol. 69, # 40 p. 8592 - 8601
参考文献
Busch; Lang
Journal fuer Praktische Chemie (Leipzig), 1936 , vol. <2> 144, p. 291,305
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Heating;
参考文献
Joseph; Jacob, Dominic E.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 2 p. 432 - 436
