反应条件
carbon disulphide in tetrahydrofuran under N2, soln. of Fe-complex in THF added to CS2 at room temp., after 30 s Re-complex (molar ratio 1.5:1) added, stirred for ca. 30 min; evapd. to dryness, residue chromd. (silica gel column, light petroleum-benzene), second yellow fraction heated in refluxing n-hexane, cooled to-10°C; elem. anal.;
参考文献
Busetto, Luigi; Palazzi, Antonio; Monari, Magda
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 1631 - 1634