反应条件
tri-n-octylamine; hydrochloric acid in water; toluene High Pressure; soln. of (NOct3H)ReO4 (mixt. of N(C8H17)3 and H2O is treated with 37percent hydrochloric acid, KReO4 added, stirring at room temp. (2 h), extn. (toluene), washed (H2O), dried (CaCl2)) in autoclave pressurized with CO (100 atm, room temp., 15 h, 100°C); autoclave pressurized with 100 atm of CO, heated (30 h, 270°C), solvent removed (vac.), pentane added, soln. cooled to -30°C, filtn., dried (vac.);
参考文献
Calderazzo, Fausto; Mazzi, Ulderico; Pampaloni, Guido; Poli, Rinaldo; Tisato, Francesco; Zanazzi, Pier Francesco
Gazzetta Chimica Italiana, 1989 , vol. 119, # 4 p. 241 - 248
