反应条件
in o-xylene Ar-atmosphere; addn. of 1.6 equiv. Cp2Ni to Re-complex, refluxing (4 h); filtration off of Re2(CO)10, concn. (60°C/0.1 Torr), chromy. (Al2O3, hexane/benzene=4:1), concn. (60°C/0.1 Torr), crystn. (-5°C, 24 h), decantation, washing (cold pentane), drying (Ar-flow, room temp.);
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 38, p. 423 - 432
Zhurnal Neorganicheskoi Khimii, , vol. 38, p. 455 - 465